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Paper 3: Required practical 5 - Distillation of a reaction product

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Total cards: 3•Content version: v4•Public deck•Updated: 8/1/2026

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#1
Front (Question)

What equipment is used for distillation?

Back (Answer)

• Semi-micro distillation apparatus • Quickfit apparatus (pear shaped flask, liebeg condenser, still head, stopper, receiver adaptor, thermometer and collectrion vessel)

#2
Front (Question)

Why are anti-bumping granules used in distillation?

Back (Answer)

To allow smooth boiling - preventing bubbles caused by vapour to cause upwards splashing in the flask

#3
Front (Question)

How do you isolate a liquid product?

Back (Answer)

• Use a separating funnel to isolate the organic layer from the aqueous layer • Shake the flask • Allow the layers to separate • Open the tep and run off one layer into a separate container